aInstitute of Chemistry, Vilnius University, Vilnius, Lithuania bDepartment of Organic Chemistry, Centre for Chemistry and Chemical Technology, Lund University, Lund, Sweden
Abstract:
Enantiomer separation of methyl exo-2-oxobicyclo[3.2.1]octane-6-carboxylate 2 has been achieved by liquid chromatography on swollen microcrystalline triacetylcellulose and the absolute configuration of (−)-2 and ( + )-2 assigned using circular dichroism spectra.
Document Type:
Article
Language: English
Citation:
E. Butkus, U. Berg, A. Stoncius, A. Zilinskas, “Chromatographic Separation and Absolute Configuration of Chiral Methyl 2-Oxobicyclo[3.2.1]octane-6-carboxylate”, Mendeleev Commun., 5:3 (1995), 96–97
Linking options:
https://www.mathnet.ru/eng/mendc5047
https://www.mathnet.ru/eng/mendc/v5/i3/p96
This publication is cited in the following 4 articles:
T. Yu. Baranova, N. V. Averina, N. V. Zyk, N. S. Zefirov, K. A. Lyssenko, M. Yu. Antipin, O. N. Zefirova, “Synthesis of indole derivatives fused with bicyclo[3.2.1]octane framework”, Mendeleev Commun., 19:1 (2009), 10–11
Sigitas Stončius, Ulf Berg, Eugenius Butkus, “Chiral bicyclic keto lactones: determination of the absolute configuration by the study of chiroptical properties and chemical correlation”, Tetrahedron: Asymmetry, 15:15 (2004), 2405
Eugenius Butkus, Ulf Berg, Albinas Žilinskas, Rytis Kubilius, Sigitas Stončius, “Enantiomer separation and absolute configuration of densely functionalized 2-oxatricyclo[4.3.1.03,8]decanes by CD spectroscopy and chemical correlation”, Tetrahedron: Asymmetry, 11:15 (2000), 3053
Ulf Berg, Eugenius Butkus, Torbjörn Frejd, Sara Bromander, “Stereochemical studies of bicyclo[5.3.1]undecane-8,11-dione. Conformational analysis, enantiomer separation, CD-spectroscopy and enolization”, Tetrahedron, 53:14 (1997), 5339
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