Abstract:
A single crystal X-ray structure of the novel layered hydrate 18-crown-6·12H2O with the following crystallographic parameters: a = 9.385(2), b = 7.399(1) c = 19.437(4), β = 93.29(3) (T = –100 °C), space group Pn, Z = 2, pcalc = 1.184 g cm–3, is reported.
Document Type:
Article
Language: English
Citation:
K. A. Udachin, J. Lipkowski, “Layered polyhydrate 18-crown-6·12H2O”, Mendeleev Commun., 6:4 (1996), 133–134
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https://www.mathnet.ru/eng/mendc4947
https://www.mathnet.ru/eng/mendc/v6/i4/p133
This publication is cited in the following 10 articles:
M. Dhanalakshmi, C. Balakrishnan, M. Vijayasri, G. Vinitha, S. Parthiban, “Synthesis, structure, third-order nonlinear optical properties and Hirshfeld surface analysis of 18-crown-6 with dimethylpyridin-1-ium iodide isomers”, Solid State Sciences, 157 (2024), 107704
A. Manikandan, M. Dhanalakshmi, L. Guganathan, T. Kokila, M. Santhamoorthy, R. Markkandan, S.C. Kim, C. Balakrishnan, “Synthesis, structural characterization and Hirshfeld surface analysis of C H···O hydrogen-bonded supramolecular complexes of 18-crown-6 with imidazolinium derivatives”, Journal of Molecular Structure, 1254 (2022), 132395
C. Balakrishnan, M. Manonmani, S. Rafi Ahamed, G. Vinitha, S. P. Meenakshisundaram, R. M. Sockalingam, “Supramolecular cocrystals of O—H...O hydrogen-bonded 18-crown-6 with isophthalic acid derivatives: Hirshfeld surface analysis and third-order nonlinear optical properties”, Acta Crystallogr B Struct Sci Cryst Eng Mater, 76:2 (2020), 241
Nikita A. Kovalenko, Elizaveta A. Pustovgar, Irina A. Uspenskaya, “The Water–18-Crown-6 System: Experimental Investigation and Thermodynamic Modeling”, J. Chem. Eng. Data, 58:1 (2013), 159
N. A. Kovalenko, N. B. Golovina, A. G. Bogachev, I. A. Uspenskaya, “Phase equilibria in water-(1-, 2-, iso-)butanol-18-crown-6 systems”, Russ. J. Phys. Chem., 85:9 (2011), 1570
E.A. Pustovgar, S.N. Igumnov, M.A. Kiskin, I.A. Uspenskaya, “Structure and properties of congruent melting 18-crown-6 crystalline hydrates”, Thermochimica Acta, 510:1-2 (2010), 154
Christof Suchentrunk, Thomas Roßmeier, Nikolaus Korber, “Crystal structures of the [18]-crown-6 ammoniate C12H24O6 · 2 NH3 and the cryptand [2.2.2] ammoniate C18H36O6N2 · 2 NH3”, Zeitschrift für Kristallographie - Crystalline Materials, 221:2 (2006), 162
K. A. Udachin, J. Lipkowski, “Water-fluorine chains in (18-crown-6)·NH4F·3H2O hydrate”, J Struct Chem, 46:S1 (2005), S84
Wansheng You, Enbo Wang, Hong Zhang, Lin Xu, Yibo Wang, “Synthesis and structural characterization of a new supermolecular compound: H 3 PW 12 O 40 ·6C 14 H 20 O 5 ·16H 2 O (C 14 H 20 O 5 =benzo-15-crown-5)”, Journal of Molecular Structure, 554:2-3 (2000), 141
K. A. Udachin, J. Lipkowski, “Layered polyhydrate 15-crown-5·8H20”, Mendeleev Commun., 6:5 (1996), 197–198
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