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Fizika Tverdogo Tela, 2017, Volume 59, Issue 6, Pages 1173–1182
DOI: https://doi.org/10.21883/FTT.2017.06.44490.230
(Mi ftt9557)
 

This article is cited in 3 scientific papers (total in 3 papers)

Phase transitions

Formation of new structural states in compressed BaTiO3 nanopowders

I. M. Shmyt'ko, D. D. Frolov, A. S. Aronin, G. R. Ganeeva, V. V. Kedrov

Institute of Solid State Physics, Russian Academy of Sciences, Chernogolovka, Moscow region
Abstract: The structural changes in BaTiO3 nanocrystal powder and tablets have been probed via X-ray diffraction, scanning electron and transmission microscopy, and differential calorimetry after successive hightemperature annealing in air. It is shown that, beginning with the annealing temperature of 1200C, significant amount of the Ba2TiO4 phase forms in the tablets together with the BaTiO3 phase. This phase is equilibrium one; it practically vanishes when the annealing temperature decreases to 700–600C; and this phase practically restored to the initial state when the annealing temperature is again increased to 1200C. Annealing the powders causes no formation of new phases, but an increase in their crystallite sizes. A probable reason of the emergence of Ba2TiO4 phase in tablets and its absence in free powder is discussed, as well.
Received: 06.06.2016
Revised: 07.12.2016
English version:
Physics of the Solid State, 2017, Volume 59, Issue 6, Pages 1196–1205
DOI: https://doi.org/10.1134/S1063783417060269
Bibliographic databases:
Document Type: Article
Language: Russian
Citation: I. M. Shmyt'ko, D. D. Frolov, A. S. Aronin, G. R. Ganeeva, V. V. Kedrov, “Formation of new structural states in compressed BaTiO3 nanopowders”, Fizika Tverdogo Tela, 59:6 (2017), 1173–1182; Phys. Solid State, 59:6 (2017), 1196–1205
Citation in format AMSBIB
\Bibitem{ShmFroAro17}
\by I.~M.~Shmyt'ko, D.~D.~Frolov, A.~S.~Aronin, G.~R.~Ganeeva, V.~V.~Kedrov
\paper Formation of new structural states in compressed BaTiO$_{3}$ nanopowders
\jour Fizika Tverdogo Tela
\yr 2017
\vol 59
\issue 6
\pages 1173--1182
\mathnet{http://mi.mathnet.ru/ftt9557}
\crossref{https://doi.org/10.21883/FTT.2017.06.44490.230}
\elib{https://elibrary.ru/item.asp?id=29405125}
\transl
\jour Phys. Solid State
\yr 2017
\vol 59
\issue 6
\pages 1196--1205
\crossref{https://doi.org/10.1134/S1063783417060269}
Linking options:
  • https://www.mathnet.ru/eng/ftt9557
  • https://www.mathnet.ru/eng/ftt/v59/i6/p1173
  • This publication is cited in the following 3 articles:
    1. Saiwei Luan, Pengfei Wang, Lei Zhang, Yanmei He, Xiong Huang, Gang Jian, Cuicui Liu, Shuhui Yu, Rong Sun, Xiuhua Cao, Zhenxiao Fu, “Atmospherically hydrothermal assisted solid-state reaction synthesis of ultrafine BaTiO3 powder with high tetragonality”, J Electroceram, 50:4 (2023), 97  crossref
    2. I. M. Shmyt'ko, “Study of changes in the crystal structure of BaTiO<sub>3</sub> under the effect of X-ray radiation”, Zavod. lab., Diagn. mater., 86:11 (2020), 36  crossref
    3. Ming Li, Lulu Gu, Tao Li, Shiji Hao, Furui Tan, Deliang Chen, Deliang Zhu, Yongjun Xu, Chenghua Sun, Zhenyu Yang, “TiO2-Seeded Hydrothermal Growth of Spherical BaTiO3 Nanocrystals for Capacitor Energy-Storage Application”, Crystals, 10:3 (2020), 202  crossref
    Citing articles in Google Scholar: Russian citations, English citations
    Related articles in Google Scholar: Russian articles, English articles
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