Аннотация:
2,6-Dimethylglycoluril 1 crystallises to form a conglomerate (space group P21) and co-crystallises with isomeric 2,8-dimethylglycoluril 2; 2,6-diethylglycoluril A is the best precursor in the synthesis of chiral drugs.
Тип публикации:
Статья
Язык публикации: английский
Образец цитирования:
R. G. Kostyanovsky, K. A. Lyssenko, A. N. Kravchenko, O. V. Lebedev, G. K. Kadorkina, V. R. Kostyanovsky, “Crystal properties of N-alkyl-substituted glycolurils as the precursors of chiral drugs”, Mendeleev Commun., 11:4 (2001), 134–136
Образцы ссылок на эту страницу:
https://www.mathnet.ru/rus/mendc4257
https://www.mathnet.ru/rus/mendc/v11/i4/p134
Эта публикация цитируется в следующих 37 статьяx:
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S. Yu. Panshina, O. V. Ponomarenko, A. A. Bakibaev, V. S. Malkov, “ANALYSIS OF XRD STRUCTURAL PARAMETERS OF GLYCOLURIL AND ITS DERIVATIVES”, J Struct Chem, 61:9 (2020), 1315
Evgeniy V. Ivanov, Elena Yu Lebedeva, “On the similarity in some thermodynamic properties of N-dimethylureas and their bis-derivatives as solutes in water”, Journal of Molecular Liquids, 310 (2020), 113134
Evgeniy V. Ivanov, Elena Yu Lebedeva, Dmitriy V. Batov, Vladimir V. Baranov, Angelina N. Kravchenko, “Equimolecular cocrystal of cis- and trans-coordinated N,N′-dimethylglycolurils: Some standard thermodynamic properties in the aqueous solution between 278.15 K and 318.15 K”, Journal of Molecular Liquids, 297 (2020), 111891
M. V. Zlokazov, K. K. Pivnitsky, “Lamellar conglomerates”, Mendeleev Commun., 30:1 (2020), 1–6
Vladimir V. Baranov, Anastasiya A. Baganova, Ilya E. Chikunov, Valentina A. Karnoukhova, Angelina N. Kravchenko, “Unexpected formation of novel two-component gels comprising of glycoluril carboxylic acid amides and imidazole: Synthesis and morphology”, Tetrahedron Letters, 60:17 (2019), 1174
V. P. Kislyi, Ya. V. Zubavichus, K. K. Babievsky, V. N. Khrustalev, K. K. Pivnitsky, “Racemic estrone methyl ether is the lamellar conglomerate”, Mendeleev Commun., 29:3 (2019), 256–259
Evgeniy V. Ivanov, “Standard Volumetric Properties of Chiral N-Methyl-Substituted Glycolurils in Water between 278.15 and 318.15 K at Ambient Pressure”, J. Chem. Eng. Data, 63:8 (2018), 2766
Evgeniy V. Ivanov, Dmitriy V. Batov, “Thermochemistry of dissolution of cis-N-dimethylglycoluril in water at T=(278.15–313.15) K and ambient pressure”, Thermochimica Acta, 625 (2016), 53
Evgeniy V. Ivanov, Dmitriy V. Batov, Angelina N. Kravchenko, “(D 2 O–H 2 O) solvent isotope effects on some thermodynamic properties of the Albicar dissolution (hydration) between T = (278.15 and 313.15) K at ambient pressure”, The Journal of Chemical Thermodynamics, 97 (2016), 341
Evgeniy V. Ivanov, Elena Yu. Lebedeva, “Standard volumetric characteristics of N-dimethyl-substituted bicyclic bisureas (glycolurils) in water at T= (278.15 to 318.15) K and p 0.1 MPa”, Journal of Molecular Liquids, 222 (2016), 1164
Evgeniy V. Ivanov, Dmitriy V. Batov, Vladimir V. Baranov, Angelina N. Kravchenko, “Temperature-dependent thermochemical properties of the Mebicaret (2,4-dimethyl-6,8-diethylglycoluril) solutions in H2O and D2O at the ambient pressure”, Thermochimica Acta, 627-629 (2016), 48
Evgeniy V. Ivanov, Elena Yu. Lebedeva, Vladimir K. Abrosimov, “Standard Volumetric Properties of Tetra-N-ethylglycoluril (Bicaret) in Ordinary and Heavy Water at Temperatures from (278.15 to 318.15) K and Ambient Pressure”, J. Chem. Eng. Data, 60:7 (2015), 2079
Evgeniy V. Ivanov, Dmitriy V. Batov, “Enthalpies and heat capacities of solution of racemic N-methyl-substituted glycolurils in water at T=(278.15 to 313.15)K”, Thermochimica Acta, 620 (2015), 59
Evgeniy V. Ivanov, Dmitriy V. Batov, Vladimir V. Baranov, Angelina N. Kravchenko, Vladimir K. Abrosimov, “Standard enthalpies and heat capacities of solution of 2,4-dimethyl- and 2,4-diethylglycolurils in water at temperatures from (278.15 to 313.15)K”, Thermochimica Acta, 586 (2014), 72
Feng Wu, Vijaybabu Mandadapu, Anthony I. Day, “Bi(OTf)3—a mild catalyst for the synthesis of difficult to obtain C-alkyl substituted glycolurils”, Tetrahedron, 69:47 (2013), 9957
Sangram Gore, Sundarababu Baskaran, Burkhard Koenig, “Synthesis of Pyrimidopyrimidinediones in a Deep Eutectic Reaction Mixture”, Adv Synth Catal, 354:13 (2012), 2368
Denis A. Lenev, Konstantin A. Lyssenko, Remir G. Kostyanovsky, “The chiral drug Albicar: resolution of its racemate via complexation with BINOL”, New J. Chem., 34:3 (2010), 403
Emiliana D'Oria, Panagiotis G. Karamertzanis, Sarah L. Price, “Spontaneous Resolution of Enantiomers by Crystallization: Insights from Computed Crystal Energy Landscapes”, Crystal Growth & Design, 10:4 (2010), 1749
A. N. Kravchenko, K. A. Lyssenko, I. E. Chikunov, P. A. Belyakov, M. M. Il'in, V. V. Baranov, Yu. V. Nelyubina, V. A. Davankov, T. S. Pivina, N. N. Makhova, M. Yu. Antipin, “4,5-Dihydroxyimidazolidin-2-ones in the α-ureidoalkylation reaction of N-(carboxyalkyl)-, N-(hydroxyalkyl)-, and N-(aminoalkyl)ureas 1. α-Ureidoalkylation of N-(carboxyalkyl)ureas”, Russ Chem Bull, 58:2 (2009), 395
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