Аннотация:
A new synthesis of 4-aryl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylic acid esters is based on the reactions of α-tosyl-substituted phenyl carbamates with the enolates of β-oxoesters followed by treatment with ammonia and dehydration of the resulting 4-hydroxyhexahydropyrimidin-2-ones.
Тип публикации:
Статья
Язык публикации: английский
Образец цитирования:
A. D. Shutalev, N. N. Kurochkin, “A new approach to the synthesis of Biginelli compounds”, Mendeleev Commun., 15:2 (2005), 70–72
Образцы ссылок на эту страницу:
https://www.mathnet.ru/rus/mendc3680
https://www.mathnet.ru/rus/mendc/v15/i2/p70
Эта публикация цитируется в следующих 12 статьяx:
Oleh Lukianov, Viktor Tkachuk, Svitlana Shishkina, Leonid Lachmann, Olga Vadzyuk, Petro Borysko, Dmytro Kovalskyy, Isabelle Gillaizeau, Volodymyr Sukach, “Hydroaminoalkyl Functionalization of Pyrimidin‐2(1H)‐ones by Visible Light Organophotocatalysis: A Radical Approach to Biginelli‐Type Dihydropyrimidines”, Adv Synth Catal, 365:20 (2023), 3484
Enrico Marcantoni, Alessandro Palmieri, Marino Petrini, “Recent synthetic applications of α-amido sulfones as precursors of N-acylimino derivatives”, Org. Chem. Front., 6:13 (2019), 2142
Anastasia A. Fesenko, Alexander N. Yankov, Anatoly D. Shutalev, “A general and convenient synthesis of 4-(tosylmethyl)semicarbazones and their use in amidoalkylation of hydrogen, heteroatom, and carbon nucleophiles”, Tetrahedron, 75:45 (2019), 130527
Anastasia A. Fesenko, Mikhail S. Grigoriev, Anatoly D. Shutalev, “A convenient stereoselective access to novel 1,2,4-triazepan-3-ones/thiones via reduction or reductive alkylation of 7-membered cyclic semicarbazones and thiosemicarbazones”, Org. Biomol. Chem., 16:43 (2018), 8072
Anastasia A. Fesenko, Anatoly D. Shutalev, 22nd International Electronic Conference on Synthetic Organic Chemistry, 2018, 14
Ludmila A. Trafimova, Maxim O. Zimin, Anatoly D. Shutalev, “Thiocarbamate-Based Synthesis of 2,4,5,6-Tetrahydro-3H-1,2,4-Triazepine-3-Thiones”, Journal of Chemical Research, 41:3 (2017), 149
Anastasia A. Fesenko, Alexander N. Yankov, Anatoly D. Shutalev, “An efficient and stereoselective approach to 14-membered hexaaza macrocycles using novel semicarbazone-based amidoalkylation reagents”, Tetrahedron Letters, 57:51 (2016), 5784
Anastasia A. Fesenko, Mikhail S. Grigoriev, Anatoly D. Shutalev, “Synthesis of aryl substituted 2,4,5,6-tetrahydro-3H-1,2,4-triazepine-3-thiones/ones starting from chalcone-derived β-isothiocyanato ketones”, Tetrahedron, 72:49 (2016), 7952
Anastasia A. Fesenko, Anatoly D. Shutalev, “Different modes of acid-catalyzed cyclization of 4-(γ-oxoalkyl)semicarbazide hydrazones: 7-membered versus 14-membered cyclic semicarbazones formation”, Tetrahedron, 71:51 (2015), 9528
Anatoly D. Shutalev, Anastasia A. Fesenko, Olesya M. Kuzmina, Alexander N. Volov, Dmitry V. Albov, Vladimir V. Chernyshev, Ilia A. Zamilatskov, “Synthesis of novel 14-membered cyclic bis-semicarbazones”, Tetrahedron Letters, 55:40 (2014), 5481
Anastasia A. Fesenko, Anatoly D. Shutalev, “A novel access to pyrido[4,3-d]pyrimidine scaffold via Staudinger/intramolecular aza-Wittig reaction of 5-acyl-4-(β-azidoalkyl)-1,2,3,4-tetrahydropyrimidin-2-ones”, Tetrahedron, 70:35 (2014), 5398
Anatoly D. Shutalev, Nikolay N. Kurochkin, “A New Approach to the Synthesis of Biginelli Compounds.”, ChemInform, 36:36 (2005)
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