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Communications DBU as a scaffold for the synthesis of [1,3]oxazolo[2’ ,3’ : 2,3]pyrimido-[1,2-a ]azepines: annulation with aromatic cyanopropargylic alcohols O. A. Shemyakina a O. G. Volostnykh a A. V. Stepanov a A. G. Mal'kina a I. A. Ushakov a K. A. Apartsin bc V. V. Kireeva c B. A. Trofimov a a A.E. Favorsky Irkutsk Institute of Chemistry, Siberian Branch of the Russian Academy of Sciences, Irkutsk, Russian Federation b Irkutsk Scientific Center of Surgery and Traumatology, Irkutsk, Russian Federation
c Biomedical Research and Technology Department of the Irkutsk Scientific Center, Siberian Branch of the Russian Academy of Sciences, Irkutsk, Russian Federation
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Аннотация:
Organic superbase DBU, 1,8-diazabicyclo[5.4.0]undec-7-ene, readily annulated with aromatic cyanopropargylic alcohols nder mild conditions (CH2 Cl2 , 20–25 °C, 30 min) to afford new cyanomethylideneperhydro[1,3]oxazolo[2’ ,3’ :2,3]pyrimido-,2-a ]azepines.
Образец цитирования:
O. A. Shemyakina, O. G. Volostnykh, A. V. Stepanov, A. G. Mal'kina, I. A. Ushakov, K. A. Apartsin, V. V. Kireeva, B. A. Trofimov, “DBU as a scaffold for the synthesis of [1,3]oxazolo[2’ ,3’ : 2,3]pyrimido-[1,2-a ]azepines: annulation with aromatic cyanopropargylic alcohols”, Mendeleev Commun. , 28 :2 (2018), 128–130
Образцы ссылок на эту страницу:
https://www.mathnet.ru/rus/mendc1686 https://www.mathnet.ru/rus/mendc/v28/i2/p128
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