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Pisma v Zhurnal Tekhnicheskoi Fiziki, 2019, Volume 45, Issue 18, Pages 52–54
DOI: https://doi.org/10.21883/PJTF.2019.18.48240.17899 (Mi pjtf5326) 		 
Mass-spectrometric observation of С$^{+}$ ions during electrospray with in-source atomization

A. A. D'yachenkoa, N. M. Blashenkovb, N. S. Samsonovab, L. N. Gall'a, A. A. Semenovc, A. V. Lizunovc, N. R. Gall'b

a Institute for Analytical Instrumentation, Russian Academy of Sciences, St. Petersburg
b Ioffe Institute, St. Petersburg
c A.A. Bochvar All-Russia Advanced Research Institute for Inorganic Materials, Moscow, Russia
Full-text PDF (99 kB)
DOI: https://doi.org/10.21883/PJTF.2019.18.48240.17899
Abstract: Carbon С$^{+}$ ions formed in a mass-spectrometric electrospray source with controlled in-source fragmentation and atomization interface have been observed for the first time. The measurements were performed in a special MI-20 LowMass mass spectrometer (MS-Bio LLC) using aqueous methanol solutions of lithium and beryllium salts. The peak of С$^{+}$ ions was substantially broadened as compared to the peaks of metal ions. A model is proposed that explains the formation of С$^{+}$ ions due to charge exchange immediately at the high-vacuum boundary near the skimmer output.
Keywords: electrospray ionization, mass spectrometry, elemental analysis, gasdynamic interface.
Received: 31.05.2019
Revised: 10.06.2019
Accepted: 14.06.2019
English version:
Technical Physics Letters, 2019, Volume 45, Issue 9, Pages 955–957
DOI: https://doi.org/10.1134/S1063785019090220
Bibliographic databases:
Document Type: Article
Language: Russian
Citation: A. A. D'yachenko, N. M. Blashenkov, N. S. Samsonova, L. N. Gall', A. A. Semenov, A. V. Lizunov, N. R. Gall', “Mass-spectrometric observation of С$^{+}$ ions during electrospray with in-source atomization”, Pisma v Zhurnal Tekhnicheskoi Fiziki, 45:18 (2019), 52–54; Tech. Phys. Lett., 45:9 (2019), 955–957
Citation in format AMSBIB
\Bibitem{DyaBlaSam19}
\by A.~A.~D'yachenko, N.~M.~Blashenkov, N.~S.~Samsonova, L.~N.~Gall', A.~A.~Semenov, A.~V.~Lizunov, N.~R.~Gall'
\paper Mass-spectrometric observation of С$^{+}$ ions during electrospray with in-source atomization
\jour Pisma v Zhurnal Tekhnicheskoi Fiziki
\yr 2019
\vol 45
\issue 18
\pages 52--54
\mathnet{http://mi.mathnet.ru/pjtf5326}
\crossref{https://doi.org/10.21883/PJTF.2019.18.48240.17899}
\elib{https://elibrary.ru/item.asp?id=41175090}
\transl
\jour Tech. Phys. Lett.
\yr 2019
\vol 45
\issue 9
\pages 955--957
\crossref{https://doi.org/10.1134/S1063785019090220}
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