|
Problemy Fiziki, Matematiki i Tekhniki (Problems of Physics, Mathematics and Technics), 2020, Issue 3(44), Pages 7–12
(Mi pfmt720)
|
|
|
|
This article is cited in 1 scientific paper (total in 1 paper)
PHYSICS
Structure formation of SiO$_2$-xerogels containing copper compounds of different phase composition
M. F. S. H. Al'-Kamali, A. A. Alekseenko, O. A. Titenkov P.O. Sukhoi Gomel State Technical University
Abstract:
Technological methods of formation of pure and composite materials of composition SiO$_2$, SiO$_2$:Cu(NO$_3$)$_2\cdot$3H$_2$O, SiO$_2$:CuO and SiO$_2$:Cu$^\circ$, obtained on the basis of an aqueous dispersion of pyrogenic silica (aerosil) grade A-300, are considered. The
method of scanning electron microscopy (SEM) was used to study the structural transformations occurring in the synthesized
xerogel blanks during their heat treatment in air and in an environment of dried hydrogen (up to $T = 800^\circ$ С). By the method of
uniaxial pressing on the basis of xerogels of the developed composition, tableted samples were formed in the form of disks with
an initial diameter of about $13$ mm, for which the arising linear shrinkage and weight loss were established in the temperature
range of $25$–$1200^\circ$ С.
Keywords:
aerosil, aqueous dispersion, sol-gel technology, structuring heat treatment, surface morphology, micropowders.
Received: 23.06.2020
Citation:
M. F. S. H. Al'-Kamali, A. A. Alekseenko, O. A. Titenkov, “Structure formation of SiO$_2$-xerogels containing copper compounds of different phase composition”, PFMT, 2020, no. 3(44), 7–12
Linking options:
https://www.mathnet.ru/eng/pfmt720 https://www.mathnet.ru/eng/pfmt/y2020/i3/p7
|
Statistics & downloads: |
Abstract page: | 73 | Full-text PDF : | 108 | References: | 10 |
|