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Nanosystems: Physics, Chemistry, Mathematics, 2019, Volume 10, Issue 2, Pages 206–214
DOI: https://doi.org/10.17586/2220-8054-2019-10-2-206-214 (Mi nano434) 		 
This article is cited in 14 scientific papers (total in 14 papers)

CHEMISTRY AND MATERIAL SCIENCE

Formation of rhabdophane-structured lanthanum orthophosphate nanoparticles in an impinging-jets microreactor and rheological properties of sols based on them

O. V. Proskurinaab, E. V. Sivtsova, M. O. Enikeevaba, A. A. Sirotkina, R. Sh. Abieva, V. V. Gusarovb

a Saint Petersburg State Institute of Technology, Moskovsky Pr., 26, Saint Petersburg, 190013, Russia
b Ioffe Institute, Politekhnicheskaya Saint 26, Saint Petersburg, 194021, Russia
Full-text PDF (7630 kB) Citations (14)
DOI: https://doi.org/10.17586/2220-8054-2019-10-2-206-214
Abstract: A free impinging-jets microreactor was used for synthesizing rhabdophane-structured LaPO$_4$ sols. The rheological behavior was investigated for the sols obtained both by reagents mixing in a microreactor, and by pouring the initial solutions together and mixing them on a magnetic stirrer. Lanthanum phosphate sols obtained by two ways are structured systems characterized by deformation behavior accompanied by shear liquefaction. Some discovered anomalies were found to be associated with flow nonequilibrium at low shear rates, which indirectly indicates stronger binding of particles in the structure of samples obtained by the microreactor synthesis.
Keywords: LaPO$_4\cdot$H$_2$O, rhabdophane, nanorods, free impinging-jets microreactor, rheology.
Funding agency Grant number
Russian Foundation for Basic Research 18-29-12119_мк
This work was supported by the Russian Foundation for Basic Research (project No 18-29-12119).
Received: 02.03.2019
Revised: 19.03.2019
Bibliographic databases:
Document Type: Article
Language: English
Citation: O. V. Proskurina, E. V. Sivtsov, M. O. Enikeeva, A. A. Sirotkin, R. Sh. Abiev, V. V. Gusarov, “Formation of rhabdophane-structured lanthanum orthophosphate nanoparticles in an impinging-jets microreactor and rheological properties of sols based on them”, Nanosystems: Physics, Chemistry, Mathematics, 10:2 (2019), 206–214
Citation in format AMSBIB
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\by O.~V.~Proskurina, E.~V.~Sivtsov, M.~O.~Enikeeva, A.~A.~Sirotkin, R.~Sh.~Abiev, V.~V.~Gusarov
\paper Formation of rhabdophane-structured lanthanum orthophosphate nanoparticles in an impinging-jets microreactor and rheological properties of sols based on them
\jour Nanosystems: Physics, Chemistry, Mathematics
\yr 2019
\vol 10
\issue 2
\pages 206--214
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\crossref{https://doi.org/10.17586/2220-8054-2019-10-2-206-214}
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