M.-x. Xu, K.-M. Zhang, “Rongalite-promoted transition metal-free synthesis of S-aryl phosphorothioates”, Mendeleev Commun., 32:3 (2022), 390

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Mendeleev Communications, 2022, Volume 32, Issue 3, Pages 390–392
DOI: https://doi.org/10.1016/j.mencom.2022.05.033 (Mi mendc674)

This article is cited in 4 scientific papers (total in 4 papers)

Communications

Rongalite-promoted transition metal-free synthesis of S-aryl phosphorothioates

M.-x. Xu^a, K.-M. Zhang^ab

^a Jiangsu Police Institute, Nanjing, P.R. China
^b Nanjing Institute of Technology, Nanjing, P.R. China

Full-text PDF (197 kB) Citations (4)

DOI: https://doi.org/10.1016/j.mencom.2022.05.033

Graphic abstract: Rongalite-promoted transition metal-free synthesis of <i>S</i>-aryl phosphorothioates

Abstract: The improved procedure for the synthesis of S-aryl phosphorothioates from dialkyl phosphites (H-phosphonates), aryl iodides and elemental sulfur deals with the application of rongalite (sodium hydroxy-methanesulfinate) as the radical promoter. The reactions proceeded smoothly to give S-aryl phosphorothioates in good yields.

Keywords: rongalite, phosphorothioates, arylation, radical process, aryl halides, sulfur.

Document Type: Article

Language: English

*Supplementary materials:*
		Supplementary_data_1.pdf	(1.3 Mb)

Citation: M.-x. Xu, K.-M. Zhang, “Rongalite-promoted transition metal-free synthesis of S-aryl phosphorothioates”, Mendeleev Commun., 32:3 (2022), 390–392

Linking options:

https://www.mathnet.ru/eng/mendc674

https://www.mathnet.ru/eng/mendc/v32/i3/p390

This publication is cited in the following 4 articles:

Li-Hua Yang, Lin Chen, Bei Li, Yuan-Xin Jin, Yun Liu, Sha Peng, Long-Yong Xie, “Synthesis of S-alkyl phosphorothioates/phosphorodithioates via ring-opening reaction of sulfonium salts with S8, H-phosphonates or P4S10, and alcohols”, Org. Chem. Front., 11:20 (2024), 5731
Rashid Ali, “Recent Developments in Rongalite Chemistry: A Critical Review”, ChemistrySelect, 8:42 (2023)
Huai‐Yu Wang, Xiang‐Long Chen, Yan‐Dong Wu, An‐Xin Wu, “Rongalite as a Versatile Reagent in Organic Synthesis†”, Chin. J. Chem., 41:23 (2023), 3388
M.-x. Xu, K.-M. Zhang, “Rongalite-promoted synthesis of β-keto sulfones via radical cascade reaction”, Mendeleev Commun., 32:5 (2022), 627–628

Citing articles in Google Scholar: Russian citations, English citations
Related articles in Google Scholar: Russian articles, English articles

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