Abstract:
The synthesis and properties of novel high-dense energetic material based on new 4H,8H-bis(furazano)[3,4-b:3',4'-e]-pyridine ring system are described. An operationally simple, efficient and scalable protocol towards 4H,8H-bis(furazano)-[3,4-b:3',4'-e]pyridin-8-one 1,7-dioxide from commercially available 4-amino-2,6-dichloropyridine in three steps, namely, nitration–azidation–cascade ring closure, has been developed.
Citation:
R. Z. Gilmanov, V. G. Nikitin, F. G. Khayrutdinov, K. V. Strizhenko, K. Yu. Suponitsky, A. B. Sheremetev, “Bis(furazano)pyridinone N,N'-dioxide: a new high-density insensitive explosive”, Mendeleev Commun., 32:1 (2022), 114–116
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https://www.mathnet.ru/eng/mendc589
https://www.mathnet.ru/eng/mendc/v32/i1/p114
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V. P. Zelenov, I. L. Dalinger, A. A. Anisimov, K. Yu. Suponitsky, A. N. Pivkina, A. B. Sheremetev, “New heterocyclic furazano[3,4-d ][1,2,3]triazine system as a platform for energetic compound engineering”, Mendeleev Commun., 32:6 (2022), 717–719
A. A. Larin, L. L. Fershtat, “Energetic heterocyclic N-oxides: synthesis and performance”, Mendeleev Commun., 32:6 (2022), 703–713
Kyrill Yu. Suponitsky, Ivan V. Fedyanin, Valentina A. Karnoukhova, Vladimir A. Zalomlenkov, Alexander A. Gidaspov, Vladimir V. Bakharev, Aleksei B. Sheremetev, “Energetic Co-Crystal of a Primary Metal-Free Explosive with BTF. Ideal Pair for Co-Crystallization”, Molecules, 26:24 (2021), 7452
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