Abstract:
The reaction of 1,3,4-trimethylglycoluril, aliphatic aldehydes and triphenyl phosphite in the presence of methanesulfonic acid affords new phosphorus-containing derivatives of glycoluril. The thus formed diastereomers of 1-[1-(diphenoxy-phosphoryl)alkyl]-3,4,6-trimethylglycolurils were separated by reverse-phase HPLC
Citation:
S. I. Gorbin, A. A. Bakibaev, D. A. Kurgachev, V. S. Malkov, K. Yu. Novolokov, G. O. Sysoev, “Synthesis of 1-[1-(diphenoxyphosphoryl)alkyl]-3,4,6-trimethylglycolurils”, Mendeleev Commun., 33:5 (2023), 638–639
Linking options:
https://www.mathnet.ru/eng/mendc480
https://www.mathnet.ru/eng/mendc/v33/i5/p638
This publication is cited in the following 3 articles:
V. V. Baranov, M. M. Antonova, S. A. Aksenova, N. G. Kolotyrkina, A. N. Kravchenko, Mendeleev Commun., 35:1 (2025), 27–30
Zhihui Yang, Xiaochen Wang, Yuanrong Wang, Jinyun Yang, Haifeng Lu, “A novel route for the synthesis of phosphonate-containing siloxanes by the catalyst-free Kabachnik—Fields reaction”, Russ Chem Bull, 73:9 (2024), 2725
Sergey I. Gorbin, Abdigali A. Bakibaev, Vera P. Tuguldurova, Andrey V. Kotov, Gleb O. Sysoev, Andrei S. Potapov, Dmitry I. Pavlov, Victor S. Malkov, Alexey S. Knyazev, Dmitriy A. Kurgachev, Mark V. Michalchenkov, “Synthesis of Novel Phosphorus-Containing Derivatives of 1,3,4-Trimethylglycoluril via the Birum–Oleksyszyn Reaction”, IJMS, 24:23 (2023), 17082
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