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Mendeleev Communications, 2024, Volume 34, Issue 1, Pages 51–53
DOI: https://doi.org/10.1016/j.mencom.2024.01.015 (Mi mendc40) 		 
This article is cited in 2 scientific papers (total in 2 papers)

Communications

A new efficient synthesis of Pyrphos ligand

Yu. N. Kononevicha, A. D. Volodina, A. A. Korlyukova, V. K. Brela, A. M. Muzafarovab

a A.N. Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences, Moscow, Russian Federation
b N.S. Enikolopov Institute of Synthetic Polymeric Materials, Russian Academy of Sciences, Moscow, Russian Federation
Full-text PDF (496 kB) Citations (2)
DOI: https://doi.org/10.1016/j.mencom.2024.01.015
Abstract: A new efficient synthesis of racemic (R*,R*)-Pyrphos ligand based on aza-Michael addition reaction of 2,3-bis(diphenylphosphoryl)buta-1,3-diene with ammonia followed by the reduction of resulting 3,4-bis(diphenylphosphoryl)pyrrolidine is proposed. The starting reactants are available but-2-yne-1,4-diol and chloro(diphenyl)phosphine.
Keywords: Pyrphos, aza-Michael addition, intramolecular cyclization, reduction, phosphines, X-ray analysis.
Document Type: Article
Language: English
Supplementary materials:
Supplementary_data_1.pdf (1.4 Mb)


Citation: Yu. N. Kononevich, A. D. Volodin, A. A. Korlyukov, V. K. Brel, A. M. Muzafarov, “A new efficient synthesis of Pyrphos ligand”, Mendeleev Commun., 34:1 (2024), 51–53
Linking options:
  • https://www.mathnet.ru/eng/mendc40
  • https://www.mathnet.ru/eng/mendc/v34/i1/p51
    • This publication is cited in the following 2 articles:
    1. E. E. Kim, D. S. Ionov, A. D. Volodin, A. A. Korlyukov, Yu. N. Kononevich, V. K. Brel, Mendeleev Commun., 35:1 (2025), 42–44  mathnet  crossref
    2. Asim Kumar, Joy Mukhopadhyay, Srikant Bhagat, “Phosphorus Heterocycles and Their Biological Applications”, ChemistrySelect, 9:45 (2024)  crossref
    Citing articles in Google Scholar: Russian citations, English citations
    Related articles in Google Scholar: Russian articles, English articles
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