Abstract:
Using enantioselective gas chromatography and X-ray diffraction analysis, we found that compound 2 forms a conglomerate (space group P21212), whereas, according to X-ray diffraction data, compound 3 crystallises as a racemic compound (space group Pccn).
Document Type:
Article
Language: English
Citation:
P. A. Levkin, K. A. Lyssenko, V. Schurig, R. G. Kostyanovsky, “A new conglomerate in a series of 2,3:6,7-dibenzobicyclo[3.3.1]nonanes”, Mendeleev Commun., 13:3 (2003), 106–108
Linking options:
https://www.mathnet.ru/eng/mendc3977
https://www.mathnet.ru/eng/mendc/v13/i3/p106
This publication is cited in the following 6 articles:
D. P. Gerasimova, E. Sh. Saigitbatalova, D. R. Islamov, D. V. Zakharychev, A. F. Saifina, A. R. Kurbangalieva, O. A. Lodochnikova, “REPRODUCIBILITY OF A HOMOCHIRAL HYDROGEN-BONDED CHAIN IN CONGLOMERATE AND RACEMIC COMPOUND CRYSTALS OF THE TRIAZOLE DERIVATIVE OF 3-PYRROLINE-2-ONE”, J Struct Chem, 63:9 (2022), 1434
Olga A. Lodochnikova, Aigul R. Zaripova, Robert R. Fayzullin, Aida I. Samigullina, Irina I. Vandyukova, Lubov N. Potapova, Almira R. Kurbangalieva, ““Doubly enantiophobic” behavior during crystallization of racemic 1,5-dihydro-2H-pyrrol-2-one thioether”, CrystEngComm, 20:23 (2018), 3218
Congfa He, Bin Wang, Mingli Gao, Zhenhua Gu, “Synthesis of Chiral Cleft C,N-Palladium and Iridium Complexes from 2,3:6,7-Dibenzobicyclo[3.3.1]nona-2,6-diene-4,8-dione and Their Synthetic Applications”, Organometallics, 36:5 (2017), 1073
O. A. Lodochnikova, Yu. K. Voronina, L. Z. Latypova, D. B. Krivolapov, A. R. Kurbangalieva, I. A. Litvinov, “Crystallization of racemic 4-arylsulfonyl-2(5H)-furanones: reproducibility of homochiral associates, conditions for the spontaneous resolution of enantiomers and the formation of racemic compounds, the role of intermolecular interactions”, Russ Chem Bull, 62:5 (2013), 1218
Claire E. Rye, David Barker, “Asymmetric Synthesis of (+)-Galbelgin, (-)-Kadangustin J, (-)-Cyclogalgravin and (-)-Pycnanthulignenes A and B, Three Structurally Distinct Lignan Classes, Using a Common Chiral Precursor”, J. Org. Chem., 76:16 (2011), 6636
Christian Roussel, Nicolas Vanthuyne, Jean‐Laurent Jobert, Andrei I. Loas, Anca E. Tanase, Dragos Gherase, “HPLC on chiral support with polarimetric detection: Application to conglomerate discovery”, Chirality, 19:6 (2007), 497
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