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Mendeleev Communications, 2014, Volume 24, Issue 3, Pages 173–175
DOI: https://doi.org/10.1016/j.mencom.2014.04.017
(Mi mendc2514)
 

This article is cited in 13 scientific papers (total in 13 papers)

Communications

Regioselective synthesis of 2,8-disubstituted 1,5-diphenylglycolurils

V. V. Baranova, M. M. Antonovaa, Yu. V. Nelyubinab, N. G. Kolotyrkinaa, I. E. Zaninc, A. N. Kravchenkoa, N. N. Makhovaa

a N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation
b A.N. Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences, Moscow, Russian Federation
c Department of Chemistry, Voronezh State University, Voronezh, Russian Federation
Abstract: A new synthetic approach to 2,8-disubstituted 1,5-diphenylglycolurils is based on condensation of 1-(hydroxyalkyl)ureas (ureido alcohols) with tetrahydroimidazooxazolone and tetrahydroimidazooxazinone derivatives which were unexpectedly obtained by acid-catalyzed reaction of ureido alcohols with benzil. An X-ray diffraction study of the supramolecular organization of the obtained compounds revealed the chirality of the crystals of achiral glycoluril molecules.
Document Type: Article
Language: English
Supplementary materials:
Supplementary_data_1.pdf (701.5 Kb)


Citation: V. V. Baranov, M. M. Antonova, Yu. V. Nelyubina, N. G. Kolotyrkina, I. E. Zanin, A. N. Kravchenko, N. N. Makhova, “Regioselective synthesis of 2,8-disubstituted 1,5-diphenylglycolurils”, Mendeleev Commun., 24:3 (2014), 173–175
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  • https://www.mathnet.ru/eng/mendc/v24/i3/p173
  • This publication is cited in the following 13 articles:
    Citing articles in Google Scholar: Russian citations, English citations
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