Abstract:
Reaction of 1-amino-2-nitroguanidine with alkyl 3-bromo-3-nitropropenoates affords 3-nitroimino-6-nitromethyl-4,5-dihydro-(2H)-1,2,4-triazin-5-one, whose structure was characterized by IR, UV, NMR spectroscopy and X-ray single crystal analysis.
Document Type:
Article
Language: English
Citation:
V. M. Berestovitskaya, O. Yu. Ozerova, T. P. Efimova, V. V. Gurzhiy, T. A. Novikova, “A new synthesis of a nitroimino-containing 1,2,4-triazin-5-one from 3-bromo-3-nitropropenoates”, Mendeleev Commun., 26:4 (2016), 323–325
Linking options:
https://www.mathnet.ru/eng/mendc2201
https://www.mathnet.ru/eng/mendc/v26/i4/p323
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Rong Wang, Yaoyao Linghu, Kai Zhong, Chaoyang Zhang, “Understanding of the difference in packing density of some energetic isomers”, CrystEngComm, 25:42 (2023), 5951
V. V. Pelipko, I. A. Pilipenko, K. A. Gomonov, R. I. Baichurin, K. A. Lyssenko, S. V. Makarenko, “Semicarbazones of alkyl 3-nitropyruvates: Synthesis and structural features”, Mendeleev Commun., 33:5 (2023), 723–725
V. V. Pelipko, K. A. Gomonov, I. A. Litvinov, R. I. Baichurin, S. V. Makarenko, “Reaction of alkyl 3-bromo-3-nitroacrylates with substituted hydrazines. Synthesis of N′-substituted alkyl 3-nitropyruvate hydrazones”, Russ Chem Bull, 71:4 (2022), 740
M. A. Kuritsyna, V. V. Pelipko, O. N. Kataeva, R. I. Baichurin, K. D. Sadikov, A. S. Smirnov, S. V. Makarenko, “Ethyl 3-halo-3-nitroacrylates: synthesis and reactions with primary aromatic amines”, Russ Chem Bull, 70:8 (2021), 1605
Vasilii V. Pelipko, Kirill A. Gomonov, “Formation of five- and six-membered nitrogen-containing heterocycles on the basis of hydrazones derived from α-dicarbonyl compounds (microreview)”, Chem Heterocycl Comp, 57:6 (2021), 624
R. I. Baichurin, K. A. Lyssenko, K. S. Kovalenko, S. V. Makarenko, “Synthesis and structure of new β-functionalized gem-bromonitroethenes — 2-arylsulfanyl- and 2-aryloxy-3-bromo-3-nitroacrylates”, Russ Chem Bull, 69:11 (2020), 2191
O. Yu. Ozerova, T. P. Efimova, T. A. Novikova, “Synthesis of 5-Substituted N-Nitro-2,4-dihydro-3H-1,2,4-triazol-3-imines”, Russ J Gen Chem, 90:8 (2020), 1403
Jinghua Wang, Meng Cai, Fengqi Zhao, Kangzhen Xu, “A Review on the Reactivity of 1-Amino-2-Nitroguanidine (ANQ)”, Molecules, 24:19 (2019), 3616
S. V. Makarenko, V. V. Pelipko, M. M. Pavchenko, R. I. Baichurin, “Alkyl 3-Bromo-3-nitroacrylates in Reactions with Aliphatic Alcohols”, Russ J Gen Chem, 89:3 (2019), 532
O. Yu. Ozerova, T. P. Efimova, T. A. Novikova, “Synthesis of New Nitroamino-Containing 1,2,4-Triazines by Reaction of 1-Amino-2-nitroguanidine with α-Diketones”, Russ J Gen Chem, 88:7 (2018), 1381
Valentina M. Berestovitskaya, Olga Yu. Ozerova, Tatiana P. Efimova, Vladislav V. Gurzhiy, Tamara A. Novikova, “ChemInform Abstract: A New Synthesis of a Nitroimino‐Containing 1,2,4‐Triazin‐5‐one from 3‐Bromo‐3‐nitropropenoates.”, ChemInform, 47:51 (2016)
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