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Mendeleev Communications, 2020, Volume 30, Issue 2, Pages 177–179
DOI: https://doi.org/10.1016/j.mencom.2020.03.015 (Mi mendc1139) 		 
This article is cited in 5 scientific papers (total in 5 papers)

Communications

Synthesis and properties of the salts of 1-nitropropan-2-one and 1-nitrobutan-2-one

V. L. Rusinovab, R. A. Drokina, D. V. Tiufiakova, E. K. Voinkova, E. N. Ulomskyab

a Institute of Chemical Engineering, Ural Federal University, Ekaterinburg, Russian Federation
b I.Ya. Postovsky Institute of Organic Synthesis, Ural Branch of the Russian Academy of Sciences, Ekaterinburg, Russian Federation
Full-text PDF (552 kB) Citations (5)
DOI: https://doi.org/10.1016/j.mencom.2020.03.015
Abstract: A new safe synthesis of α-nitro ketone salts via alkaline hydrolysis of 2-morpholino-1-nitroalkenes has been developed. The salts were introduced into the reactions of diazotization and heterocyclization. Crystal structures of new 2-morpholino-1-nitrobut-1-ene and 6-ethyl-5-nitro-4phenyl-3,4-dihydropyrimidin-2-one have been determined.
Keywords: nitro compounds, ketones, nitroazine systems, nitroacetone, enamines, diazonium salts, pyrimidinones, hydrazones.
Document Type: Article
Language: English
Supplementary materials:
Supplementary_data_1.pdf (1.9 Mb)


Citation: V. L. Rusinov, R. A. Drokin, D. V. Tiufiakov, E. K. Voinkov, E. N. Ulomsky, “Synthesis and properties of the salts of 1-nitropropan-2-one and 1-nitrobutan-2-one”, Mendeleev Commun., 30:2 (2020), 177–179
Linking options:
  • https://www.mathnet.ru/eng/mendc1139
  • https://www.mathnet.ru/eng/mendc/v30/i2/p177
    • This publication is cited in the following 5 articles:
    1. D. N. Lyapustin, V. V. Fedotov, E. N. Ulomsky, V. L. Rusinov, O. N. Chupakhin, “Recent advances in the chemistry of two-carbon nitro-containing synthetic equivalents”, Russian Chem. Reviews, 92:4 (2023), RCR5077  mathnet  mathnet  crossref  isi  scopus
    2. Daniil N. Lyapustin, Svetlana K. Kotovskaya, Ilya I. Butorin, Evgeny N. Ulomsky, Vladimir L. Rusinov, Denis A. Babkov, Alexander A. Pokhlebin, Alexander A. Spasov, Vsevolod V. Melekhin, Maria D. Tokhtueva, Anna V. Shcheglova, Oleg G. Makeev, “CK2 Inhibition and Antitumor Activity of 4,7-Dihydro-6-nitroazolo[1,5-a]pyrimidines”, Molecules, 27:16 (2022), 5239  crossref
    3. Roman A. Drokin, Dmitrii V. Tiufiakov, Egor K. Voinkov, Pavel A. Slepukhin, Evgeny N. Ulomsky, Yana L. Esaulkova, Alexandrina S. Volobueva, Kristina S. Lantseva, Mariya A. Misyurina, Vladimir V. Zarubaev, Vladimir L. Rusinov, “Methods of Synthesis and Antiviral Activity of New 4-Alkyl-3-Nitro-1,4-Dihydroazolo[5,1-c][1,2,4]Triazin-4-ols”, Chem Heterocycl Comp, 57:4 (2021), 473  crossref
    4. Daniil N. Lyapustin, Evgeny N. Ulomsky, Ilya A. Balyakin, Alexander V. Shchepochkin, Vladimir L. Rusinov, Oleg N. Chupakhin, “Oxidative Aromatization of 4,7-Dihydro-6-nitroazolo[1,5-a]pyrimidines: Synthetic Possibilities and Limitations, Mechanism of Destruction, and the Theoretical and Experimental Substantiation”, Molecules, 26:16 (2021), 4719  crossref
    5. Daniil N. Lyapustin, Evgeny N. Ulomsky, Vladimir L. Rusinov, “6-Nitro-4,7-dihydroazolo [1,5-a]pyrimidines: an alternative mechanism of formation and studies of alkylation”, Chem Heterocycl Comp, 56:11 (2020), 1465  crossref
    Citing articles in Google Scholar: Russian citations, English citations
    Related articles in Google Scholar: Russian articles, English articles
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