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Zhurnal Tekhnicheskoi Fiziki, 2018, Volume 88, Issue 11, Pages 1743–1751
DOI: https://doi.org/10.21883/JTF.2018.11.46639.32-18
(Mi jtf5781)
 

Physical electronics

Spectroscopic investigation of the evolution of fractal nanoobjects in film-forming sols of orthosilicic acid

I. A. Averina, S. E. Igoshinaa, A. A. Karmanova, I. A. Proninab, V. A. Moshnikovab, E. I. Terukovc

a Penza State University
b Saint Petersburg Electrotechnical University "LETI"
c Ioffe Institute, St. Petersburg
Abstract: The evolution of fractal nanoparticles of medium size and concentration, which are formed and dynamically change during hydrolytic polycondensation, has been investigated using IR spectroscopy. It is shown that the application of the Smoluchowski rapid coagulation model combined with analysis of the characteristic absorption line intensity in the IR spectra provides a satisfactory estimate of evolution processes occurring in sols of orthosilisic acid. The obtained spectroscopic dependences are compared qualitatively with atomic force microscopy data.
Keywords: Film-forming Sols, Orthosilicic Acid, Hydrolytic Polycondensation, Nanoparticle Fraction, AFM Data.
Funding agency Grant number
Ministry of Education and Science of the Russian Federation 16.897.2017/4.6
СП-3800.2018.1
Received: 18.01.2018
English version:
Technical Physics, 2018, Volume 63, Issue 11, Pages 1687–1695
DOI: https://doi.org/10.1134/S106378421811004X
Bibliographic databases:
Document Type: Article
Language: Russian
Citation: I. A. Averin, S. E. Igoshina, A. A. Karmanov, I. A. Pronin, V. A. Moshnikov, E. I. Terukov, “Spectroscopic investigation of the evolution of fractal nanoobjects in film-forming sols of orthosilicic acid”, Zhurnal Tekhnicheskoi Fiziki, 88:11 (2018), 1743–1751; Tech. Phys., 63:11 (2018), 1687–1695
Citation in format AMSBIB
\Bibitem{AveIgoKar18}
\by I.~A.~Averin, S.~E.~Igoshina, A.~A.~Karmanov, I.~A.~Pronin, V.~A.~Moshnikov, E.~I.~Terukov
\paper Spectroscopic investigation of the evolution of fractal nanoobjects in film-forming sols of orthosilicic acid
\jour Zhurnal Tekhnicheskoi Fiziki
\yr 2018
\vol 88
\issue 11
\pages 1743--1751
\mathnet{http://mi.mathnet.ru/jtf5781}
\crossref{https://doi.org/10.21883/JTF.2018.11.46639.32-18}
\elib{https://elibrary.ru/item.asp?id=36904551}
\transl
\jour Tech. Phys.
\yr 2018
\vol 63
\issue 11
\pages 1687--1695
\crossref{https://doi.org/10.1134/S106378421811004X}
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