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Zhurnal Tekhnicheskoi Fiziki, 2019, Volume 89, Issue 9, Pages 1406–1411
DOI: https://doi.org/10.21883/JTF.2019.09.48067.437-18 (Mi jtf5519) 		 
This article is cited in 2 scientific papers (total in 2 papers)

Physics of nanostructures

Analysis of the structural evolution of zinc oxide powders obtained by mechanical high-energy grinding

I. A. Averina, I. A. Proninab, N. D. Yakushovaa, A. A. Karmanova, M. M. Sychovcd, S. V. Vikhmanc, V. S. Levitskiie, V. A. Moshnikovab, E. I. Terukovf

a Penza State University
b Saint Petersburg Electrotechnical University "LETI"
c State Technological Institute of St. Petersburg (Technical University)
d I. V. Grebenshchikov Institute of Silicate Chemistry of the Russian Academy of Sciences, St. Petersburg
e Research and Development Center for Thin-Film Technologies in Energetics, St. Petersburg, Russia
f Ioffe Institute, St. Petersburg
Full-text PDF (1103 kB) Citations (2)
DOI: https://doi.org/10.21883/JTF.2019.09.48067.437-18
Abstract: Zinc oxide powders made by mechanical high-energy grinding have been investigated using the methods of scanning electron microscopy, thermal nitrogen desorption, and Raman spectroscopy of infrared Fourier spectroscopy. Their structural evolution, including reduction of the average size of crystallites, increase in specific surface area, as well as changes in the number and ratio of adsorption centers, has been demonstrated. The data on the reconstruction of the surface of zinc oxide powders and multiple bond breaking in near-surface areas resulting from long-term dispersion have been presented.
Keywords: zinc oxide, grinding, attritor, Fourier-transform IR spectroscopy, Raman spectroscopy.
Funding agency Grant number
Ministry of Education and Science of the Russian Federation 16.897.2017/ПЧ
СП-84.2018.1
СП-3800.2018.1
МК-1882.2018.8
The work was received financial support from the Ministry of Education and Science of the Russian Federation (project 16.897.2017/PCh), as well as Scholarships and Grants of the President of the Russian Federation (SP-84.2018.1, SP-3800.2018.1, MK-1882.2018.8).
Received: 22.12.2018
Revised: 22.12.2018
Accepted: 25.03.2019
English version:
Technical Physics, 2019, Volume 64, Issue 9, Pages 1330–1335
DOI: https://doi.org/10.1134/S1063784219090020
Bibliographic databases:
Document Type: Article
Language: Russian
Citation: I. A. Averin, I. A. Pronin, N. D. Yakushova, A. A. Karmanov, M. M. Sychov, S. V. Vikhman, V. S. Levitskii, V. A. Moshnikov, E. I. Terukov, “Analysis of the structural evolution of zinc oxide powders obtained by mechanical high-energy grinding”, Zhurnal Tekhnicheskoi Fiziki, 89:9 (2019), 1406–1411; Tech. Phys., 64:9 (2019), 1330–1335
Citation in format AMSBIB
\Bibitem{AveProYak19}
\by I.~A.~Averin, I.~A.~Pronin, N.~D.~Yakushova, A.~A.~Karmanov, M.~M.~Sychov, S.~V.~Vikhman, V.~S.~Levitskii, V.~A.~Moshnikov, E.~I.~Terukov
\paper Analysis of the structural evolution of zinc oxide powders obtained by mechanical high-energy grinding
\jour Zhurnal Tekhnicheskoi Fiziki
\yr 2019
\vol 89
\issue 9
\pages 1406--1411
\mathnet{http://mi.mathnet.ru/jtf5519}
\crossref{https://doi.org/10.21883/JTF.2019.09.48067.437-18}
\elib{https://elibrary.ru/item.asp?id=41130904}
\transl
\jour Tech. Phys.
\yr 2019
\vol 64
\issue 9
\pages 1330--1335
\crossref{https://doi.org/10.1134/S1063784219090020}
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