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Zhurnal Tekhnicheskoi Fiziki, 2021, Volume 91, Issue 2, Pages 287–290
DOI: https://doi.org/10.21883/JTF.2021.02.50364.203-20
(Mi jtf5082)
 

This article is cited in 9 scientific papers (total in 9 papers)

Physical science of materials

X-ray photoelectron spectroscopy of nanodiamonds obtained by grinding and detonation synthesis

P. P. Sharina, A. V. Sivtsevaa, V. I. Popovb

a Institute of Physico-Engineering Problems of the North of the Siberian Division of RAS
b North-Eastern Federal University named after M. K. Ammosov, Yakutsk, Russia
Full-text PDF (617 kB) Citations (9)
Abstract: The chemical composition and surface state of nanopowder particles prepared by milling natural diamond and detonation synthesis were studied by the method of X-ray photoelectron spectroscopy. It has been shown that the primary particles of both nanopowders contain mainly carbon and oxygen atoms. The signals in the photoelectronic spectrum from atoms of nitrogen, sulfur, chlorine and metals do not exceed the noise level. It was found that in primary particles of detonation synthesis nanodiamond and nanopowder obtained by grinding natural diamond, the proportions of carbon atoms in the $sp^3$ hybridization state are $\sim$46.5 and $\sim$67.8%, $sp^2$ hybridization is $\sim$26.8 and $\sim$17.4% and in the composition of oxygen-containing functional groups $\sim$26.7 and $\sim$14.7%, respectively.
Keywords: milling, XPS method, elemental composition and chemical state of the surface of nanodiamonds, oxygen-containing functional groups.
Received: 15.06.2020
Revised: 18.08.2020
Accepted: 24.08.2020
English version:
Technical Physics, 2021, Volume 66, Issue 2, Pages 275–279
DOI: https://doi.org/10.1134/S1063784221020183
Bibliographic databases:
Document Type: Article
Language: Russian
Citation: P. P. Sharin, A. V. Sivtseva, V. I. Popov, “X-ray photoelectron spectroscopy of nanodiamonds obtained by grinding and detonation synthesis”, Zhurnal Tekhnicheskoi Fiziki, 91:2 (2021), 287–290; Tech. Phys., 66:2 (2021), 275–279
Citation in format AMSBIB
\Bibitem{ShaSivPop21}
\by P.~P.~Sharin, A.~V.~Sivtseva, V.~I.~Popov
\paper X-ray photoelectron spectroscopy of nanodiamonds obtained by grinding and detonation synthesis
\jour Zhurnal Tekhnicheskoi Fiziki
\yr 2021
\vol 91
\issue 2
\pages 287--290
\mathnet{http://mi.mathnet.ru/jtf5082}
\crossref{https://doi.org/10.21883/JTF.2021.02.50364.203-20}
\elib{https://elibrary.ru/item.asp?id=44885095}
\transl
\jour Tech. Phys.
\yr 2021
\vol 66
\issue 2
\pages 275--279
\crossref{https://doi.org/10.1134/S1063784221020183}
\scopus{https://www.scopus.com/record/display.url?origin=inward&eid=2-s2.0-85101885710}
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  • This publication is cited in the following 9 articles:
    Citing articles in Google Scholar: Russian citations, English citations
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