Abstract:
The density of coarse-crystalline and nanocrystalline powders of niobium carbide NbCy (0.77 ⩽y⩽ 0.96) (with a different average particle sizes of 3–5 μm and 60–30 nm, respectively) was measured by helium pycnometry. The nanopowders were obtained via the high-energy ball milling of initial coarse-crystalline niobium carbide powders. The particle size of niobium carbide powders was estimated by X-ray diffraction and the Brunauer–Emmet–Taylor (BET) method. The nanopowder density measured by helium pycnometry was shown to be underestimated in comparison with the true density due to the adsorption of helium by the highly developed surface of carbide nanopowders.
Citation:
A. S. Kurlov, A. I. Gusev, “Density and particle size of cubic niobium carbide NbCy nanocrystalline powders”, Fizika Tverdogo Tela, 59:1 (2017), 176–182; Phys. Solid State, 59:1 (2017), 184–190
\Bibitem{KurGus17}
\by A.~S.~Kurlov, A.~I.~Gusev
\paper Density and particle size of cubic niobium carbide NbC$_y$ nanocrystalline powders
\jour Fizika Tverdogo Tela
\yr 2017
\vol 59
\issue 1
\pages 176--182
\mathnet{http://mi.mathnet.ru/ftt9727}
\crossref{https://doi.org/10.21883/FTT.2017.01.43971.182}
\elib{https://elibrary.ru/item.asp?id=28969450}
\transl
\jour Phys. Solid State
\yr 2017
\vol 59
\issue 1
\pages 184--190
\crossref{https://doi.org/10.1134/S106378341701019X}
Linking options:
https://www.mathnet.ru/eng/ftt9727
https://www.mathnet.ru/eng/ftt/v59/i1/p176
This publication is cited in the following 2 articles:
Sarmad Naim Katea, Cheuk-Wai Tai, Per-Olof Larsson, Hilmar Vidarsson, Gunnar Westin, “Nickel dot coating of NbC powder by solution processing”, Open Ceramics, 4 (2020), 100043
Igor L. Shabalin, Ultra-High Temperature Materials II, 2019, 249