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Fizika Tverdogo Tela, 2018, Volume 60, Issue 2, Pages 383–389
DOI: https://doi.org/10.21883/FTT.2018.02.45397.240
(Mi ftt9316)
 

Low dimensional systems

Anomalous dependence of the intensity of X-ray reflections of Cs$_{2}$SO$_{4}$ on the crystallite size and shape

I. M. Shmyt'ko, V. V. Kedrov, A. S. Aronin

Institute of Solid State Physics, Russian Academy of Sciences, Chernogolovka, Moscow region
Abstract: Detailed X-ray and electron microscopy analyses of Cs$_{2}$SO$_{4}$ powders consisting of sphere- and platelike crystallites have been carried out. It is established that the intensity distributions of X-ray reflections in both cases radically differ, with the position on the diffraction-angle axis retained in accordance with the PDF-2 database. Electron microscopy microdiffraction investigations of the orientation of developed surfaces of platelike crystallites revealed four different directions; however, these directions could not provide texture amplification of a number of observed $(hkl)$ reflections. It is suggested that the intensity redistribution is based on the sphericity of X-ray waves incident on the sample.
Received: 18.07.2017
English version:
Physics of the Solid State, 2018, Volume 60, Issue 2, Pages 390–396
DOI: https://doi.org/10.1134/S1063783418020269
Bibliographic databases:
Document Type: Article
Language: Russian
Citation: I. M. Shmyt'ko, V. V. Kedrov, A. S. Aronin, “Anomalous dependence of the intensity of X-ray reflections of Cs$_{2}$SO$_{4}$ on the crystallite size and shape”, Fizika Tverdogo Tela, 60:2 (2018), 383–389; Phys. Solid State, 60:2 (2018), 390–396
Citation in format AMSBIB
\Bibitem{ShmKedAro18}
\by I.~M.~Shmyt'ko, V.~V.~Kedrov, A.~S.~Aronin
\paper Anomalous dependence of the intensity of X-ray reflections of Cs$_{2}$SO$_{4}$ on the crystallite size and shape
\jour Fizika Tverdogo Tela
\yr 2018
\vol 60
\issue 2
\pages 383--389
\mathnet{http://mi.mathnet.ru/ftt9316}
\crossref{https://doi.org/10.21883/FTT.2018.02.45397.240}
\elib{https://elibrary.ru/item.asp?id=32739791}
\transl
\jour Phys. Solid State
\yr 2018
\vol 60
\issue 2
\pages 390--396
\crossref{https://doi.org/10.1134/S1063783418020269}
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